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Rationale: Protic ionic liquids have the potential to be useful materials for primary ion beams in terms of protonation, since they have active protons. Selecting protic ionic liquids suitable for primary ion beams is of great importance to increase molecular secondary ion yields. Propylammonium nitrate ([C3 H7 NH3 ][NO3 ]) seems promising in view of its proton affinity. It is likely that [C3 H7 NH3 ]+ cations can act as proton donors, and [NO3 ]- anions can work as proton acceptors.
Methods: Time-of-flight secondary ion mass spectrometry (TOF-SIMS) experiments have been performed to verify the usefulness of [C3 H7 NH3 ][NO3 ]. A primary propylammonium nitrate cluster ion beam was generated by vacuum electrospray, and then used to analyze amino acids (arginine, glutamic acid, aspartic acid), angiotensin II and polyethylene glycol. Positive and negative secondary ion mass spectra were obtained to study both protonation and deprotonation.
Results: The propylammonium nitrate cluster ion beam successfully generated protonated molecules [M + H]+ of all the analytes in positive ion mode. The primary ion beam also generated deprotonated molecules [M - H]- of glutamic acid, aspartic acid and angiotensin II in negative ion mode. Additionally, adduct ions related to [C3 H7 NH3 ][NO3 ] were detected in the case of arginine and polyethylene glycol.
Conclusions: The TOF-SIMS experiments confirmed that the propylammonium nitrate cluster ion beam was useful in generating molecular secondary ions, demonstrating that it is well suited for a primary ion beam in TOF-SIMS.
Wednesday December 1The day shift began with the Antiproton Source (Pbar), Tevatron (TeV), Recycler, and MiniBooNE all conducting studies. At 1:09 PM, an attempt to raise intensity in Main Injector (MI) caused a number of vacuum bursts and vacuum valves to close.A MI expert began a three-hour slipstacking study at 2:09 PM.Operations received permission to send beam to the Switchyard dump at 2:24 PM.Operations reported the following on beamline status at 4:36 PM:Tevatron will measure and smooth orbits, and set tunes and possibly chromaticitiesSY beam is on hold due to power supply workRecycler will first work on optimizing compensation between the Recycler and MI ramps and then work on tune couplingMiniBooNE wants to take as much beam as possibleNuMI worked on getting beam through MIAt 8:44 PM, Operations reported the first of many MI trips due to vacuum bursts while trying to send beam to the SY dump.Pbar experts completed their study at 11:14 PM. During their study, they managed to stack at a rate of 4mA per hour.At 11:53 PM, the TeV began suffering from aborts at sector F2. Operators discovered a number of vacuum valves closed in the P3 line; the P3 line transfers beam from MI to SY through F sector in the TeV. Operators opened all but one of the valves from the service building.Thursday December 2The midnight shift began with Pbar conducting reverse proton studies, with TeV conducting ramp studies, and Recycler conducting studies, and with MiniBooNE taking beam.At 2:37 AM, Pbar's lithium lens tripped off. It reset okay.Pbar experts reported at 5:44 AM that they were having problems with their reverse proton study due to large beam oscillations in their transfer lines.Operators began preparing Pbar for a tunnel access at 8:43 AM.NuMI experts began a study period at 8:45 AM.The Pbar access ended and they resumed stacking at 11:31 AM.Operators prepared TeV F sector for an access at 12:36 PM.Preaccelerator experts accessed the H- Source at 12:42 PM.Cryo system technicians began work at 1:03 PM on wet engines at TeV sector B3 and C1.Operations prepared Booster for an access at 1:09 PM. They came out of access an hour and a half later.Vacuum techs reported at 2:49 PM that the TeV sector F19 valve had resumed working.Operators reported that they had interlocked NuMI at 3:28 PM.Operations resumed sending beam to MI, Pbar, and MiniBooNE at 3:38 PM.Operations began sending beam to SY at 4 PM.TeV came out of access and at 5:24 PM completed its first 980 GeV ramp. At 5:37 PM, they went into a dry squeeze. Operations established beam in the TeV at 6:06 PM.A MI expert completed her coalescing study at 7:48 PM and a NuMI expert finished his ramp study.A Recycler expert began a study at 9:36 PM.Friday December 3The midnight shift began with Pbar stacking, with the TeV, Recycler, Pbar, and SY conducting studies, and with MiniBooNE off.Pbar stacking studies ended at 1:08 AM.SY studies ended at 2 AM.Recycler studies ended at 2:41 AM.TeV experts reported at 6:08 AM that they had measured chromaticities up the ramp, but couldn't decouple the particle central orbits.Operators prepared MiniBooNE for an access at 6:30 AM.Plans for the WeekendNuMI will attempt to take beam today, 12/3/04. The plan is to continue with beam startup.Accelerator Update ArchiveMore InformationFor Tevatron luminosity charts and the current status of Fermilab'saccelerators and detectors (live!), please go to Fermilab NowComments and SuggestionsWhat do you think about the Accelerator Updates Please send comments and suggestions to: accelupdates@fnal.gov. last modified 12/3/2004 email Fermilab Fermi National Accelerator LaboratoryOffice of Science/U.S. Department of EnergyManaged by Fermi Research Alliance, LLCFermilabSecurity, Privacy, Legal Use of CookiesHomeHelpPress RoomFRLsDFx9eyfrPXgV
All clinical IMRT plans were recalculated with the MC algorithm with heterogeneity correction. Identical beam configurations and monitor unit settings were used in the recalculated plans. Parameters for the MC dose calculation were 2 mm for the spatial resolution, 2% for the mean variance, \"dose to medium\" for the dose result type, and \"accuracy optimized\" for the multileaf collimator (MLC) modeling.
For the MLD and V20 of the combined lungs, excellent correlations were observed between the MC and PB calculations (Fig. 4). For the central tumors, linear fittings resulted in the slopes of 0.998 and 0.974 for the MLD and V20 of combined lungs, respectively. For the peripheral tumors, the corresponding slopes were 0.991 for the MLD and 0.952 for V20 of the combined lungs. No significant differences were observed between the PB and MC calculations for the MLD. However, the PB calculation resulted in an average 5% overestimation of V20 for the peripheral tumors and 2.5% for the central tumors when compared to the MC calculation.
For all the organs at risk, differences in the maximum dose between the PB and MC calculations were negligible. Excellent correlations were observed for both the MLD and V20 of combined lung between the PB and MC calculations. A simple rescaling can be applied to the volume/dose endpoints when considering radiation treatment related toxicity to the lungs. Previous studies reported that PB calculations overestimated MLD by 7% when compared to MC calculations for centrally located tumors,(16) and by 5% for patients with the peripheral tumors.(9) However, no significant differences were observed between the PB and MC calculations for the MLD in our patient samples. These different results may stem from the delivery methods. Our study included IMRT plans, while other studies included 3D conformal arc plans.8, 9 59ce067264
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